Lista de obras - Francesco Gasparrini - Dominio Público Uruguay

"Quasi flexible" automatic docking processing for studying stereoselective recognition mechanisms, part 2: Prediction of DeltaDeltaG of complexation and 1H-NMR NOE correlation

artículo científico publicado en 2007

A chiral A2 B2 macrocyclic minireceptor with extreme enantioselectivity

artículo científico publicado en 2002

A general procedure for the synthesis of stereochemically pure conduritol derivatives practical also for solid-phase chemistry

artículo científico publicado en 2006

A new method to investigate the intrusion of water into porous hydrophobic structures under dynamic conditions

artículo científico publicado en 2012

A rational approach to predict and modulate stereolability of chiral alpha substituted ketones

artículo científico publicado en 2009

Absolute configuration and biological profile of two thiazinooxadiazol-3-ones with L-type calcium channel activity: a study of the structural effects

Adsorption Mechanisms in Normal-Phase Chromatography. Mobile-Phase Modifier Adsorption from Dilute Solutions and Displacement Effect

scientific article published on 19 April 2007

Adsorption equilibria of benzodiazepines on a hybrid polymeric chiral stationary phase

artículo científico publicado en 2005

An efficient route to tetrahydronaphthols via addition of ortho-lithiated stilbene oxides to alpha,beta-unsaturated fischer carbene Complexes

artículo científico publicado en 2005

An unexpected highly stereoselective bisaziridination of (E,E)-1,4-dialkyl-2,3-dinitrobutadienes followed by a nitro group driven ring enlargement.

artículo científico publicado en 2009

Analysis of bovine milk caseins on organic monolithic columns: an integrated capillary liquid chromatography-high resolution mass spectrometry approach for the study of time-dependent casein degradation

artículo científico

Application of a new chiral stationary phase containing the glycopeptide antibiotic A-40,926 in the direct chromatographic resolution of β-amino acids

article by Ilaria D’Acquarica et al published June 2000 in Tetrahedron: Asymmetry

Bidentate urea-based chiral selectors for enantioselective high performance liquid chromatography: Synthesis and evaluation of “Crab-like” stationary phases

artículo científico publicado en 2013

Binding of dipeptides and amino acids to Teicoplanin chiral stationary phase: apparent homogeneity of some heterogeneous systems.

artículo científico publicado en 2009

Calcium channel antagonists discovered by a multidisciplinary approach

artículo científico publicado en 2006

Cannabis sativa L. Inflorescences from Monoecious Cultivars Grown in Central Italy: An Untargeted Chemical Characterization from Early Flowering to Ripening

artículo científico publicado en 2020

Cannabis through the looking glass: chemo- and enantio-selective separation of phytocannabinoids by enantioselective ultra high performance supercritical fluid chromatography.

artículo científico publicado en 2017

Characterization of new types of stationary phases for fast and ultra-fast liquid chromatography by signal processing based on AutoCovariance Function: a case study of application to Passiflora incarnata L. extract separations.

artículo científico publicado en 2010

Chiral azole derivatives. 4. Enantiomers of bifonazole and related antifungal agents: synthesis, configuration assignment, and biological evaluation

scientific article published on 01 July 2000

Combination of HPLC "inverted chirality columns approach" and MS/MS detection for extreme enantiomeric excess determination even in absence of reference samples. Application to camptothecin derivatives

scientific article published on 29 June 2007

Conformational studies by dynamic NMR. 89. Stereomutation and cryogenic enantioseparation of conformational antipodes of hindered aryl oximes.

artículo científico publicado en 2002

Design and evaluation of hydrolytically stable bidentate urea-type stationary phases for hydrophilic interaction chromatography

artículo científico publicado en 2011

Determination of the polarities of some ionic liquids using 2-nitrocyclohexanone as the probe

artículo científico publicado en 2005

Direct analysis of chiral active pharmaceutical ingredients and their counterions by ultra high performance liquid chromatography with macrocyclic glycopeptide-based chiral stationary phases

artículo científico publicado en 2018

Direct chromatographic resolution of carnitine and O-acylcarnitine enantiomers on a teicoplanin-bonded chiral stationary phase

artículo científico publicado en 1999

Dynamic HPLC of stereolabile iron(II) complexes on chiral stationary phases.

artículo científico publicado en 2009

Dynamic high performance liquid chromatography on chiral stationary phases. Low temperature separation of the interconverting enantiomers of diazepam, flunitrazepam, prazepam and tetrazepam.

artículo científico publicado en 2014

Efficient Thia-bridged triarylamine heterohelicenes: synthesis, resolution, and absolute configuration determination.

artículo científico publicado en 2008

Efficient enantiorecognition of ruthenium(II) complexes by silica-bound teicoplanin

scholarly article by Francesco Gasparrini et al published September 2000 in Tetrahedron: Asymmetry

Enantiomeric resolution of sulfoxides on a DACH-DNB chiral stationary phase: A quantitative structure-enantioselective retention relationship (QSERR) study

article by Cosimo Altomare et al published 1993 in Chirality

Enantiomerization study of some alpha-nitroketones by dynamic high-resolution gas chromatography

artículo científico publicado en 2003

Enantioselective liquid chromatographic-electrospray mass spectrometric assay of beta-adrenergic blockers: application to a pharmacokinetic study of sotalol in human plasma.

artículo científico publicado en 2003

Enantioselective ultra-high and high performance liquid chromatography: a comparative study of columns based on the Whelk-O1 selector

artículo científico publicado en 2012

Enantioseparation by ultra-high-performance liquid chromatography

scholarly article by Alberto Cavazzini et al published December 2014 in Trends in Analytical Chemistry

Evaluation of teicoplanin chiral stationary phases of 3.5 and 5 microm inside diameter silica microparticles by polar-organic mode capillary electrochromatography

artículo científico publicado en 2003

Evaluation of the macrocyclic glycopeptide A-40,926 as a high-performance liquid chromatographic chiral selector and comparison with teicoplanin chiral stationary phase

artículo científico publicado en 2000

Exceptional gas-phase enantioselectivity of chiral tetramide macrocycles.

artículo científico publicado en 2005

Expanding the potential of chiral chromatography for high-throughput screening of large compound libraries by means of sub-2μm Whelk-O 1 stationary phase in supercritical fluid conditions

artículo científico publicado en 2015

Extending the use of "Inverted Chirality Columns Approach" for enantiomeric excess determination in absence of reference samples: Application to a water-soluble camptothecin derivative.

artículo científico publicado en 2009

Fluorous Affinity Chromatography for Enrichment and Determination of Perfluoroalkyl Substances

artículo científico publicado en 2012

Gas-phase enantioselective reactions in noncovalent ion-molecule complexes.

artículo científico publicado en 2009

Geometric characterization of straight-chain perfluorohexylpropyl adsorbents for high performance liquid chromatography

artículo científico publicado en 2013

High barrier to rotation about the Pd–N bond in trans-dichloro-dihydrazonepalladium(II) complexes

article published in 1977

High-performance liquid chromatography chiral stationary phases based on low-molecular-mass selectors.

artículo científico publicado en 2001

Hybrid polyacrylamide chiral stationary phases for HPLC prepared by surface-initiated photopolymerization.

artículo científico publicado en 2010

Immobilized trypsin on epoxy organic monoliths with modulated hydrophilicity: novel bioreactors useful for protein analysis by liquid chromatography coupled to tandem mass spectrometry

scientific article published on 27 May 2011

Inductive and Mesomeric Effects of the [60]Fulleropyrrolidine Fragment and [60]Fullerene Sphere: A Quantitative Evaluation Based on Theory and Experiments

Internal motions in a fulleropyrrolidine tertiary amide with axial chirality

artículo científico publicado en 2004

Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase.

artículo científico publicado en 2012

Investigation of mass transfer properties and kinetic performance of high-efficiency columns packed with C18 sub-2 μm fully and superficially porous particles

artículo científico publicado en 2020

Molecular Recognition by a Silica-Bound Fullerene Derivative

article by Alberto Bianco et al published August 1997 in Journal of the American Chemical Society

N-terminal anthranoyl-phenylalanine derivatives as CCK1 receptor antagonists: the final approach

artículo científico publicado en 2005

New Anthranilic Acid Based Antagonists with High Affinity and Selectivity for the Human Cholecystokinin Receptor 1 (hCCK1-R) ⬇️

artículo científico publicado el 20 de julio de 2011

New chiral and restricted-access materials containing glycopeptides as selectors for the high-performance liquid chromatographic determination of chiral drugs in biological matrices.

artículo científico publicado en 2007

New hybrid polymeric liquid chromatography chiral stationary phase prepared by surface-initiated polymerization.

artículo científico publicado en 2005

On the effect of chiral selector loading and mobile phase composition on adsorption properties of latest generation fully- and superficially-porous Whelk-O1 particles for high-efficient ultrafast enantioseparations

On-column epimerization of dihydroartemisinin: an effective analytical approach to overcome the shortcomings of the International Pharmacopoeia monograph.

artículo científico publicado en 2008

Recognition mechanism of aromatic derivatives resolved by argentation chromatography: The driving role played by substituent groups.

artículo científico publicado en 2018

Revealing the fine details of functionalized silica surfaces by solid-state NMR and adsorption isotherm measurements: the case of fluorinated stationary phases for liquid chromatography

artículo científico publicado en 2014

Role of the carbohydrate moieties in chiral recognition on teicoplanin-based LC stationary phases

scientific article published on 01 April 2000

Separation of complex sugar mixtures on a hydrolytically stable bidentate urea-type stationary phase for hydrophilic interaction near ultra high performance liquid chromatography

artículo científico publicado en 2014

Simultaneous determination of 16 anti-HIV drugs in human plasma by high-performance liquid chromatography

artículo científico publicado en 2006

Stereodynamic investigation of labile stereogenic centres in dihydroartemisinin.

artículo científico publicado en 2010

Stereolability of dihydroartemisinin, an antimalarial drug: a comprehensive kinetic investigation. Part 2.

artículo científico publicado en 2011

Stereolability of dihydroartemisinin, an antimalarial drug: a comprehensive thermodynamic investigation. Part 1.

artículo científico publicado en 2011

Stereoselective behavior of the functional diltiazem analogue 1-[(4-chlorophenyl)sulfonyl]-2-(2-thienyl)pyrrolidine, a new L-type calcium channel blocker

artículo científico publicado en 2009

Study of mechanisms of chiral discrimination of amino acids and their derivatives on a teicoplanin-based chiral stationary phase

artículo científico publicado en 2004

Study of the Aggregation Properties of a Novel Amphiphilic C60Fullerene Derivative

article published in 2001

Substituent effects on the enantioselective retention of anti-HIV 5-aryl-delta 2-1,2,4-oxadiazolines on R,R-DACH-DNB chiral stationary phase.

artículo científico publicado en 1996

Synthesis and characterization of novel internal surface reversed-phase silica supports for high-performance liquid chromatography

artículo científico publicado en 2007

Synthesis of sugar-based silica gels by copper-catalysed azide-alkyne cycloaddition via a single-step azido-activated silica intermediate and the use of the gels in hydrophilic interaction chromatography

artículo científico publicado en 2010

Synthesis, chromatographic separation, vibrational circular dichroism spectroscopy, and ab initio DFT studies of chiral thiepane tetraol derivatives

artículo científico publicado en 2005

The "bridge" game: role of the fourth player in chiral recognition

artículo científico publicado en 2011

The dynamic chromatographic behavior of tri-o-thymotide on HPLC chiral stationary phases

artículo científico publicado en 2012

Toward enantioselective nano ultrahigh-performance liquid chromatography with Whelk-O1 chiral stationary phase

scientific article published on 14 August 2014

Towards enzyme-like enantioselectivity in the gas phase: conformational control of selectivity in chiral macrocyclic dimers.

artículo científico publicado en 2009

Transition from enantioselective high performance to ultra-high performance liquid chromatography: A case study of a brush-type chiral stationary phase based on sub-5-micron to sub-2-micron silica particles.

artículo científico publicado en 2009

Twenty years of research on silica-based chiral stationary phases

artículo científico publicado en 2006

Ultra-fast high-efficiency enantioseparations by means of a teicoplanin-based chiral stationary phase made on sub-2 μm totally porous silica particles of narrow size distribution

artículo científico publicado en 2015

Ultra-high performance separation of basic compounds on reversed-phase columns packed with fully/superficially porous silica and hybrid particles by using ultraviolet transparent hydrophobic cationic additives

scientific article published on 11 February 2020

Understanding Mixed-Mode Retention Mechanisms in Liquid Chromatography with Hydrophobic Stationary Phases

artículo científico publicado en 2014

Lista de obras de Francesco Gasparrini

"Quasi flexible" automatic docking processing for studying stereoselective recognition mechanisms, part 2: Prediction of DeltaDeltaG of complexation and 1H-NMR NOE correlation

A chiral A2 B2 macrocyclic minireceptor with extreme enantioselectivity

A general procedure for the synthesis of stereochemically pure conduritol derivatives practical also for solid-phase chemistry

A new method to investigate the intrusion of water into porous hydrophobic structures under dynamic conditions

A rational approach to predict and modulate stereolability of chiral alpha substituted ketones

Absolute configuration and biological profile of two thiazinooxadiazol-3-ones with L-type calcium channel activity: a study of the structural effects

Adsorption Mechanisms in Normal-Phase Chromatography. Mobile-Phase Modifier Adsorption from Dilute Solutions and Displacement Effect

Adsorption equilibria of benzodiazepines on a hybrid polymeric chiral stationary phase

An efficient route to tetrahydronaphthols via addition of ortho-lithiated stilbene oxides to alpha,beta-unsaturated fischer carbene Complexes

An unexpected highly stereoselective bisaziridination of (E,E)-1,4-dialkyl-2,3-dinitrobutadienes followed by a nitro group driven ring enlargement.

Analysis of bovine milk caseins on organic monolithic columns: an integrated capillary liquid chromatography-high resolution mass spectrometry approach for the study of time-dependent casein degradation

Application of a new chiral stationary phase containing the glycopeptide antibiotic A-40,926 in the direct chromatographic resolution of β-amino acids

Bidentate urea-based chiral selectors for enantioselective high performance liquid chromatography: Synthesis and evaluation of “Crab-like” stationary phases

Binding of dipeptides and amino acids to Teicoplanin chiral stationary phase: apparent homogeneity of some heterogeneous systems.

Calcium channel antagonists discovered by a multidisciplinary approach

Cannabis sativa L. Inflorescences from Monoecious Cultivars Grown in Central Italy: An Untargeted Chemical Characterization from Early Flowering to Ripening

Cannabis through the looking glass: chemo- and enantio-selective separation of phytocannabinoids by enantioselective ultra high performance supercritical fluid chromatography.

Characterization of new types of stationary phases for fast and ultra-fast liquid chromatography by signal processing based on AutoCovariance Function: a case study of application to Passiflora incarnata L. extract separations.

Chiral azole derivatives. 4. Enantiomers of bifonazole and related antifungal agents: synthesis, configuration assignment, and biological evaluation

Combination of HPLC "inverted chirality columns approach" and MS/MS detection for extreme enantiomeric excess determination even in absence of reference samples. Application to camptothecin derivatives

Conformational studies by dynamic NMR. 89. Stereomutation and cryogenic enantioseparation of conformational antipodes of hindered aryl oximes.

Design and evaluation of hydrolytically stable bidentate urea-type stationary phases for hydrophilic interaction chromatography

Determination of the polarities of some ionic liquids using 2-nitrocyclohexanone as the probe

Direct analysis of chiral active pharmaceutical ingredients and their counterions by ultra high performance liquid chromatography with macrocyclic glycopeptide-based chiral stationary phases

Direct chromatographic resolution of carnitine and O-acylcarnitine enantiomers on a teicoplanin-bonded chiral stationary phase

Dynamic HPLC of stereolabile iron(II) complexes on chiral stationary phases.

Dynamic high performance liquid chromatography on chiral stationary phases. Low temperature separation of the interconverting enantiomers of diazepam, flunitrazepam, prazepam and tetrazepam.

Efficient Thia-bridged triarylamine heterohelicenes: synthesis, resolution, and absolute configuration determination.

Efficient enantiorecognition of ruthenium(II) complexes by silica-bound teicoplanin

Enantiomeric resolution of sulfoxides on a DACH-DNB chiral stationary phase: A quantitative structure-enantioselective retention relationship (QSERR) study

Enantiomerization study of some alpha-nitroketones by dynamic high-resolution gas chromatography

Enantioselective liquid chromatographic-electrospray mass spectrometric assay of beta-adrenergic blockers: application to a pharmacokinetic study of sotalol in human plasma.

Enantioselective ultra-high and high performance liquid chromatography: a comparative study of columns based on the Whelk-O1 selector

Enantioseparation by ultra-high-performance liquid chromatography

Evaluation of teicoplanin chiral stationary phases of 3.5 and 5 microm inside diameter silica microparticles by polar-organic mode capillary electrochromatography

Evaluation of the macrocyclic glycopeptide A-40,926 as a high-performance liquid chromatographic chiral selector and comparison with teicoplanin chiral stationary phase

Exceptional gas-phase enantioselectivity of chiral tetramide macrocycles.

Expanding the potential of chiral chromatography for high-throughput screening of large compound libraries by means of sub-2μm Whelk-O 1 stationary phase in supercritical fluid conditions

Extending the use of "Inverted Chirality Columns Approach" for enantiomeric excess determination in absence of reference samples: Application to a water-soluble camptothecin derivative.

Fluorous Affinity Chromatography for Enrichment and Determination of Perfluoroalkyl Substances

Gas-phase enantioselective reactions in noncovalent ion-molecule complexes.

Geometric characterization of straight-chain perfluorohexylpropyl adsorbents for high performance liquid chromatography

High barrier to rotation about the Pd–N bond in trans-dichloro-dihydrazonepalladium(II) complexes

High-performance liquid chromatography chiral stationary phases based on low-molecular-mass selectors.

Hybrid polyacrylamide chiral stationary phases for HPLC prepared by surface-initiated photopolymerization.

Immobilized trypsin on epoxy organic monoliths with modulated hydrophilicity: novel bioreactors useful for protein analysis by liquid chromatography coupled to tandem mass spectrometry

Inductive and Mesomeric Effects of the [60]Fulleropyrrolidine Fragment and [60]Fullerene Sphere: A Quantitative Evaluation Based on Theory and Experiments

Internal motions in a fulleropyrrolidine tertiary amide with axial chirality

Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase.

Investigation of mass transfer properties and kinetic performance of high-efficiency columns packed with C18 sub-2 μm fully and superficially porous particles

Molecular Recognition by a Silica-Bound Fullerene Derivative

N-terminal anthranoyl-phenylalanine derivatives as CCK1 receptor antagonists: the final approach

New Anthranilic Acid Based Antagonists with High Affinity and Selectivity for the Human Cholecystokinin Receptor 1 (hCCK1-R) ⬇️

New chiral and restricted-access materials containing glycopeptides as selectors for the high-performance liquid chromatographic determination of chiral drugs in biological matrices.

New hybrid polymeric liquid chromatography chiral stationary phase prepared by surface-initiated polymerization.

On the effect of chiral selector loading and mobile phase composition on adsorption properties of latest generation fully- and superficially-porous Whelk-O1 particles for high-efficient ultrafast enantioseparations

On-column epimerization of dihydroartemisinin: an effective analytical approach to overcome the shortcomings of the International Pharmacopoeia monograph.

Recognition mechanism of aromatic derivatives resolved by argentation chromatography: The driving role played by substituent groups.

Revealing the fine details of functionalized silica surfaces by solid-state NMR and adsorption isotherm measurements: the case of fluorinated stationary phases for liquid chromatography

Role of the carbohydrate moieties in chiral recognition on teicoplanin-based LC stationary phases

Separation of complex sugar mixtures on a hydrolytically stable bidentate urea-type stationary phase for hydrophilic interaction near ultra high performance liquid chromatography

Simultaneous determination of 16 anti-HIV drugs in human plasma by high-performance liquid chromatography

Stereodynamic investigation of labile stereogenic centres in dihydroartemisinin.

Stereolability of dihydroartemisinin, an antimalarial drug: a comprehensive kinetic investigation. Part 2.

Stereolability of dihydroartemisinin, an antimalarial drug: a comprehensive thermodynamic investigation. Part 1.

Stereoselective behavior of the functional diltiazem analogue 1-[(4-chlorophenyl)sulfonyl]-2-(2-thienyl)pyrrolidine, a new L-type calcium channel blocker

Study of mechanisms of chiral discrimination of amino acids and their derivatives on a teicoplanin-based chiral stationary phase

Study of the Aggregation Properties of a Novel Amphiphilic C60Fullerene Derivative

Substituent effects on the enantioselective retention of anti-HIV 5-aryl-delta 2-1,2,4-oxadiazolines on R,R-DACH-DNB chiral stationary phase.

Synthesis and characterization of novel internal surface reversed-phase silica supports for high-performance liquid chromatography

Synthesis of sugar-based silica gels by copper-catalysed azide-alkyne cycloaddition via a single-step azido-activated silica intermediate and the use of the gels in hydrophilic interaction chromatography

Synthesis, chromatographic separation, vibrational circular dichroism spectroscopy, and ab initio DFT studies of chiral thiepane tetraol derivatives

The "bridge" game: role of the fourth player in chiral recognition

The dynamic chromatographic behavior of tri-o-thymotide on HPLC chiral stationary phases

Toward enantioselective nano ultrahigh-performance liquid chromatography with Whelk-O1 chiral stationary phase

Towards enzyme-like enantioselectivity in the gas phase: conformational control of selectivity in chiral macrocyclic dimers.

Transition from enantioselective high performance to ultra-high performance liquid chromatography: A case study of a brush-type chiral stationary phase based on sub-5-micron to sub-2-micron silica particles.

Twenty years of research on silica-based chiral stationary phases

Ultra-fast high-efficiency enantioseparations by means of a teicoplanin-based chiral stationary phase made on sub-2 μm totally porous silica particles of narrow size distribution