Lista de obras - Alessia Ciogli - Dominio Público Uruguay

A general procedure for the synthesis of stereochemically pure conduritol derivatives practical also for solid-phase chemistry

artículo científico publicado en 2006

A new method to investigate the intrusion of water into porous hydrophobic structures under dynamic conditions

artículo científico publicado en 2012

ABCB1 Structural Models, Molecular Docking, and Synthesis of New Oxadiazolothiazin-3-one Inhibitors.

artículo científico publicado en 2013

Absolute configuration and biological profile of two thiazinooxadiazol-3-ones with L-type calcium channel activity: a study of the structural effects

An unexpected highly stereoselective bisaziridination of (E,E)-1,4-dialkyl-2,3-dinitrobutadienes followed by a nitro group driven ring enlargement.

artículo científico publicado en 2009

Atropisomerism in 3-arylthiazolidine-2-thiones. A combined dynamic NMR and dynamic HPLC study

artículo científico publicado en 2016

Atropisomers of arylmaleimides: stereodynamics and absolute configuration

artículo científico publicado en 2013

Binding of dipeptides and amino acids to Teicoplanin chiral stationary phase: apparent homogeneity of some heterogeneous systems.

artículo científico publicado en 2009

Calcium channel antagonists discovered by a multidisciplinary approach

artículo científico publicado en 2006

Capillary methacrylate-based monoliths by grafting from/to γ-ray polymerization on a tentacle-type reactive surface for the liquid chromatographic separations of small molecules and intact proteins

artículo científico publicado en 2016

Characterization of new types of stationary phases for fast and ultra-fast liquid chromatography by signal processing based on AutoCovariance Function: a case study of application to Passiflora incarnata L. extract separations.

artículo científico publicado en 2010

Chemical, computational and functional insights into the chemical stability of the Hedgehog pathway inhibitor GANT61.

artículo científico publicado en 2018

Combination of HPLC "inverted chirality columns approach" and MS/MS detection for extreme enantiomeric excess determination even in absence of reference samples. Application to camptothecin derivatives

scientific article published on 29 June 2007

Design and evaluation of hydrolytically stable bidentate urea-type stationary phases for hydrophilic interaction chromatography

artículo científico publicado en 2011

Determination of enantiomerization barriers of hypericin and pseudohypericin by dynamic high-performance liquid chromatography on immobilized polysaccharide-type chiral stationary phases and off-column racemization experiments.

artículo científico publicado en 2010

Dynamic HPLC of stereolabile iron(II) complexes on chiral stationary phases.

artículo científico publicado en 2009

Dynamic high performance liquid chromatography on chiral stationary phases. Low temperature separation of the interconverting enantiomers of diazepam, flunitrazepam, prazepam and tetrazepam.

artículo científico publicado en 2014

Efficient Thia-bridged triarylamine heterohelicenes: synthesis, resolution, and absolute configuration determination.

artículo científico publicado en 2008

Enantioselective ultra high performance liquid and supercritical fluid chromatography: The race to the shortest chromatogram

artículo científico publicado en 2018

Enantioselective ultra-high and high performance liquid chromatography: a comparative study of columns based on the Whelk-O1 selector

artículo científico publicado en 2012

Enantioseparation by ultra-high-performance liquid chromatography

scholarly article by Alberto Cavazzini et al published December 2014 in Trends in Analytical Chemistry

Evaluation of two sub-2μm stationary phases, core–shell and totally porous monodisperse, in the second dimension of on-line comprehensive two dimensional liquid chromatography, a case study: Separation of milk peptides after expiration date

artículo científico publicado en 2014

Expanding the potential of chiral chromatography for high-throughput screening of large compound libraries by means of sub-2μm Whelk-O 1 stationary phase in supercritical fluid conditions

artículo científico publicado en 2015

Experimental evidence of the kinetic performance achievable with columns packed with new 1.9μm fully porous particles of narrow particle size distribution

artículo científico publicado en 2016

Extending the use of "Inverted Chirality Columns Approach" for enantiomeric excess determination in absence of reference samples: Application to a water-soluble camptothecin derivative.

artículo científico publicado en 2009

Future perspectives in high efficient and ultrafast chiral liquid chromatography through zwitterionic teicoplanin-based 2-μm superficially porous particles.

artículo científico publicado en 2017

Hybrid polyacrylamide chiral stationary phases for HPLC prepared by surface-initiated photopolymerization.

artículo científico publicado en 2010

Immobilized trypsin on epoxy organic monoliths with modulated hydrophilicity: novel bioreactors useful for protein analysis by liquid chromatography coupled to tandem mass spectrometry

scientific article published on 27 May 2011

Inductive and Mesomeric Effects of the [60]Fulleropyrrolidine Fragment and [60]Fullerene Sphere: A Quantitative Evaluation Based on Theory and Experiments

Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase.

artículo científico publicado en 2012

Molecular Recognition of the HPLC Whelk-O1 Selector towards the Conformational Enantiomers of Nevirapine and Oxcarbazepine

artículo científico publicado en 2020

N-terminal anthranoyl-phenylalanine derivatives as CCK1 receptor antagonists: the final approach

artículo científico publicado en 2005

New Anthranilic Acid Based Antagonists with High Affinity and Selectivity for the Human Cholecystokinin Receptor 1 (hCCK1-R) ⬇️

artículo científico publicado el 20 de julio de 2011

New chiral and restricted-access materials containing glycopeptides as selectors for the high-performance liquid chromatographic determination of chiral drugs in biological matrices.

artículo científico publicado en 2007

Novel Insights on Human Carbonic Anhydrase Inhibitors Based on Coumalic Acid: Design, Synthesis, Molecular Modeling Investigation, and Biological Studies

artículo científico publicado en 2022

On-column epimerization of dihydroartemisinin: an effective analytical approach to overcome the shortcomings of the International Pharmacopoeia monograph.

artículo científico publicado en 2008

Organocatalytic atroposelective formal Diels-Alder desymmetrization of N-arylmaleimides

artículo científico publicado en 2015

Pirkle-type chiral stationary phase on core–shell and fully porous particles: Are superficially porous particles always the better choice toward ultrafast high-performance enantioseparations?

artículo científico publicado en 2016

Rationale behind the optimum efficiency of columns packed with new 1.9μm fully porous particles of narrow particle size distribution.

artículo científico publicado en 2016

Recognition mechanism of aromatic derivatives resolved by argentation chromatography: The driving role played by substituent groups.

artículo científico publicado en 2018

Remote control of axial chirality: aminocatalytic desymmetrization of N-arylmaleimides via vinylogous Michael addition

article

Revealing the fine details of functionalized silica surfaces by solid-state NMR and adsorption isotherm measurements: the case of fluorinated stationary phases for liquid chromatography

artículo científico publicado en 2014

Separation of complex sugar mixtures on a hydrolytically stable bidentate urea-type stationary phase for hydrophilic interaction near ultra high performance liquid chromatography

artículo científico publicado en 2014

Separation of intact proteins on γ-ray-induced polymethacrylate monolithic columns: A highly permeable stationary phase with high peak capacity for capillary high-performance liquid chromatography with high-resolution mass spectrometry

artículo científico publicado en 2015

Stereolability of chiral ruthenium catalysts with frozen NHC ligand conformations investigated by dynamic-HPLC.

artículo científico publicado en 2015

Stereoselective behavior of the functional diltiazem analogue 1-[(4-chlorophenyl)sulfonyl]-2-(2-thienyl)pyrrolidine, a new L-type calcium channel blocker

artículo científico publicado en 2009

Study of mechanisms of chiral discrimination of amino acids and their derivatives on a teicoplanin-based chiral stationary phase

artículo científico publicado en 2004

Synthesis and characterization of novel internal surface reversed-phase silica supports for high-performance liquid chromatography

artículo científico publicado en 2007

Synthesis of sugar-based silica gels by copper-catalysed azide-alkyne cycloaddition via a single-step azido-activated silica intermediate and the use of the gels in hydrophilic interaction chromatography

artículo científico publicado en 2010

Tetrasubstituted cyclopentadienones as suitable enantiopure ligands with axial chirality.

artículo científico publicado en 2017

The experimental observation of the intramolecular NO₂/CO interaction in solution

artículo científico publicado en 2014

Toward enantioselective nano ultrahigh-performance liquid chromatography with Whelk-O1 chiral stationary phase

scientific article published on 14 August 2014

Transition from enantioselective high performance to ultra-high performance liquid chromatography: A case study of a brush-type chiral stationary phase based on sub-5-micron to sub-2-micron silica particles.

artículo científico publicado en 2009

Ultra-fast high-efficiency enantioseparations by means of a teicoplanin-based chiral stationary phase made on sub-2 μm totally porous silica particles of narrow size distribution

artículo científico publicado en 2015

Ultra-high performance separation of basic compounds on reversed-phase columns packed with fully/superficially porous silica and hybrid particles by using ultraviolet transparent hydrophobic cationic additives

scientific article published on 11 February 2020

Understanding Mixed-Mode Retention Mechanisms in Liquid Chromatography with Hydrophobic Stationary Phases

artículo científico publicado en 2014

Lista de obras de Alessia Ciogli

A general procedure for the synthesis of stereochemically pure conduritol derivatives practical also for solid-phase chemistry

A new method to investigate the intrusion of water into porous hydrophobic structures under dynamic conditions

ABCB1 Structural Models, Molecular Docking, and Synthesis of New Oxadiazolothiazin-3-one Inhibitors.

Absolute configuration and biological profile of two thiazinooxadiazol-3-ones with L-type calcium channel activity: a study of the structural effects

An unexpected highly stereoselective bisaziridination of (E,E)-1,4-dialkyl-2,3-dinitrobutadienes followed by a nitro group driven ring enlargement.

Atropisomerism in 3-arylthiazolidine-2-thiones. A combined dynamic NMR and dynamic HPLC study

Atropisomers of arylmaleimides: stereodynamics and absolute configuration

Binding of dipeptides and amino acids to Teicoplanin chiral stationary phase: apparent homogeneity of some heterogeneous systems.

Calcium channel antagonists discovered by a multidisciplinary approach

Capillary methacrylate-based monoliths by grafting from/to γ-ray polymerization on a tentacle-type reactive surface for the liquid chromatographic separations of small molecules and intact proteins

Characterization of new types of stationary phases for fast and ultra-fast liquid chromatography by signal processing based on AutoCovariance Function: a case study of application to Passiflora incarnata L. extract separations.

Chemical, computational and functional insights into the chemical stability of the Hedgehog pathway inhibitor GANT61.

Combination of HPLC "inverted chirality columns approach" and MS/MS detection for extreme enantiomeric excess determination even in absence of reference samples. Application to camptothecin derivatives

Design and evaluation of hydrolytically stable bidentate urea-type stationary phases for hydrophilic interaction chromatography

Determination of enantiomerization barriers of hypericin and pseudohypericin by dynamic high-performance liquid chromatography on immobilized polysaccharide-type chiral stationary phases and off-column racemization experiments.

Dynamic HPLC of stereolabile iron(II) complexes on chiral stationary phases.

Dynamic high performance liquid chromatography on chiral stationary phases. Low temperature separation of the interconverting enantiomers of diazepam, flunitrazepam, prazepam and tetrazepam.

Efficient Thia-bridged triarylamine heterohelicenes: synthesis, resolution, and absolute configuration determination.

Enantioselective ultra high performance liquid and supercritical fluid chromatography: The race to the shortest chromatogram

Enantioselective ultra-high and high performance liquid chromatography: a comparative study of columns based on the Whelk-O1 selector

Enantioseparation by ultra-high-performance liquid chromatography

Evaluation of two sub-2μm stationary phases, core–shell and totally porous monodisperse, in the second dimension of on-line comprehensive two dimensional liquid chromatography, a case study: Separation of milk peptides after expiration date

Expanding the potential of chiral chromatography for high-throughput screening of large compound libraries by means of sub-2μm Whelk-O 1 stationary phase in supercritical fluid conditions

Experimental evidence of the kinetic performance achievable with columns packed with new 1.9μm fully porous particles of narrow particle size distribution

Extending the use of "Inverted Chirality Columns Approach" for enantiomeric excess determination in absence of reference samples: Application to a water-soluble camptothecin derivative.

Future perspectives in high efficient and ultrafast chiral liquid chromatography through zwitterionic teicoplanin-based 2-μm superficially porous particles.

Hybrid polyacrylamide chiral stationary phases for HPLC prepared by surface-initiated photopolymerization.

Immobilized trypsin on epoxy organic monoliths with modulated hydrophilicity: novel bioreactors useful for protein analysis by liquid chromatography coupled to tandem mass spectrometry

Inductive and Mesomeric Effects of the [60]Fulleropyrrolidine Fragment and [60]Fullerene Sphere: A Quantitative Evaluation Based on Theory and Experiments

Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase.

Molecular Recognition of the HPLC Whelk-O1 Selector towards the Conformational Enantiomers of Nevirapine and Oxcarbazepine

N-terminal anthranoyl-phenylalanine derivatives as CCK1 receptor antagonists: the final approach

New Anthranilic Acid Based Antagonists with High Affinity and Selectivity for the Human Cholecystokinin Receptor 1 (hCCK1-R) ⬇️

New chiral and restricted-access materials containing glycopeptides as selectors for the high-performance liquid chromatographic determination of chiral drugs in biological matrices.

Novel Insights on Human Carbonic Anhydrase Inhibitors Based on Coumalic Acid: Design, Synthesis, Molecular Modeling Investigation, and Biological Studies

On-column epimerization of dihydroartemisinin: an effective analytical approach to overcome the shortcomings of the International Pharmacopoeia monograph.

Organocatalytic atroposelective formal Diels-Alder desymmetrization of N-arylmaleimides

Pirkle-type chiral stationary phase on core–shell and fully porous particles: Are superficially porous particles always the better choice toward ultrafast high-performance enantioseparations?

Rationale behind the optimum efficiency of columns packed with new 1.9μm fully porous particles of narrow particle size distribution.

Recognition mechanism of aromatic derivatives resolved by argentation chromatography: The driving role played by substituent groups.

Remote control of axial chirality: aminocatalytic desymmetrization of N-arylmaleimides via vinylogous Michael addition

Revealing the fine details of functionalized silica surfaces by solid-state NMR and adsorption isotherm measurements: the case of fluorinated stationary phases for liquid chromatography

Separation of complex sugar mixtures on a hydrolytically stable bidentate urea-type stationary phase for hydrophilic interaction near ultra high performance liquid chromatography

Separation of intact proteins on γ-ray-induced polymethacrylate monolithic columns: A highly permeable stationary phase with high peak capacity for capillary high-performance liquid chromatography with high-resolution mass spectrometry

Stereolability of chiral ruthenium catalysts with frozen NHC ligand conformations investigated by dynamic-HPLC.

Stereoselective behavior of the functional diltiazem analogue 1-[(4-chlorophenyl)sulfonyl]-2-(2-thienyl)pyrrolidine, a new L-type calcium channel blocker

Study of mechanisms of chiral discrimination of amino acids and their derivatives on a teicoplanin-based chiral stationary phase

Synthesis and characterization of novel internal surface reversed-phase silica supports for high-performance liquid chromatography

Synthesis of sugar-based silica gels by copper-catalysed azide-alkyne cycloaddition via a single-step azido-activated silica intermediate and the use of the gels in hydrophilic interaction chromatography

Tetrasubstituted cyclopentadienones as suitable enantiopure ligands with axial chirality.

The experimental observation of the intramolecular NO₂/CO interaction in solution

Toward enantioselective nano ultrahigh-performance liquid chromatography with Whelk-O1 chiral stationary phase

Transition from enantioselective high performance to ultra-high performance liquid chromatography: A case study of a brush-type chiral stationary phase based on sub-5-micron to sub-2-micron silica particles.

Ultra-fast high-efficiency enantioseparations by means of a teicoplanin-based chiral stationary phase made on sub-2 μm totally porous silica particles of narrow size distribution

Ultra-high performance separation of basic compounds on reversed-phase columns packed with fully/superficially porous silica and hybrid particles by using ultraviolet transparent hydrophobic cationic additives

Understanding Mixed-Mode Retention Mechanisms in Liquid Chromatography with Hydrophobic Stationary Phases